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  • Summary & Details

Pulsed Neutron Small Angle Scattering Combined with Dynamic Nuclear Polarization ー Neutron Microscope to Observe Industrial Product as It Is

21世紀の自動車産業の技術課題を解決する中性子小角散乱 ─製品のありのままの観察を目指して─

Detailed Information

Category(J)ホットトピックス

Translation

Category(E)Hot Topics
Author(J)1) 小泉 智, 2) 能田 洋平
Author(E)1) Satoshi Koizumi, 2) Yohei Noda
Affiliation(J)1) 茨城大学, 2) 茨城大学
Abstract(J)中性子小角散乱は原子レベルからマイクロメートルまでのさまざまなサイズの構造を観察できる分析法である。茨城大学では強磁場を利用して中性子が感じる水素の色合いを自在にコントロールできる顕微装置を開発しこの中性子小角散乱を組み合わせ、21世紀の自動車産業の様々な技術課題に取り組んでいる。

Translation

Abstract(E)We developed the novel neutron microscope on the instrument iMATERIA at MLF of J-PARC, which was originally a powder diffractometer, recently reinforced by small-angle scattering. The method of dynamic nuclear polarization (DNP) for protons was combined with small angle neutron scattering (SANS) (DNP-SANS). In a long course of history of DNP, our activity is the first challenge to incorporate DNP-SANS for routine industry uses. This "neutron microscope" provides us multiple reciprocal space images by changing scattering lengths of proton, in turn by varying "contrast" of individual scattering components. The DNP approach is suitable for industry application (for example to observe tire rubbers), because we do not need highly-specialized deuterium substitution, which has been conventional. We report the studies on vulcanized SBR rubber. We also report the studies on the polymer electrolyte fuel cell (PEFC) by using ultra-small-angle neutron scattering and/or deuterium gas contrast variation methods.

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